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PENENTUAN KONSENTRASI LARUTAN KOH TERBAIK PADA SAPONIFIKASI STEARIN HASIL PENGOLAHAN MINYAK SAWIT KASAR DI MINI PLANT POLITEKNIK KAMPAR MENGHASILKAN SABUN DAN GLISEROL

PENENTUAN KONSENTRASI LARUTAN KOH TERBAIK PADA SAPONIFIKASI STEARIN HASIL PENGOLAHAN MINYAK SAWIT KASAR DI MINI PLANT POLITEKNIK KAMPAR MENGHASILKAN
SABUN DAN GLISEROL

Fatmayati1 and  Nur Asma Deli2
1,2Program Studi Teknik Pengolahan Sawit
Jl. Tengku Muhammad (KM.2), Bangkinang, 28461

ABSTRACT


Politeknik Kampar as an educational institution based palm oil industry has a mini  plant processing crude palm oil plant with a capacity of 700 kg  / batch which produces olein and stearin. Stearin until now still not processed and utilized in order to bring economic value. The research purposes were to examine the use of stearin to produce soap and glycerol, knowing the best concentration of KOH solution on the process of saponification of palm oil stearin and produces soap and glycerol in consistent with ISO related. The preliminary research  was conducted to determine whether stearin can be saponified in order to produces soap and glycerol. Stearin saponification was carried out on a variation of the reaction time is 30; 60; 90 and 120 minutes and the variation of the concentration of KOH solution is equal to 3, 4, 5 and 6 N at a temperature of 70 OC and the stirring rate of 40 rpm. Procedures analysis of soap characteristics produced in consistent with SNI 06-3532-1994 and procedures analysis of glycerol characteristic produced in consistent with SNI 06-1564-1995. Stearin, crude palm oil processing results in mini plant Politeknik Kampar can be used to produces soap and glycerol through the saponification reaction.. The best concentration of KOH solution in the saponification process palm oil stearin was at a concentration KOH solution of 3 N.  Soap was produced from the reaction of saponification palm oil sterin had  average free fatty acid  of 0.2 and average water content of 2.15 in consistent with SNI  06-3532-1994. However, the characteristics of the resulting glycerol was not all in consistent with the relevant SNI . Only average water content of 6.59 and average ash content of 6.10 that consistent with SNI but average glycerol levels of 10.53 not consistent with SNI 06-1564-1995.


Key words : saponification, stearin, soap, glycerol.

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